This thesis touched upon the effect of iron doping on the structural, morphological, compositional, optical and dielectric properties of bismuth oxide thin films. Bismuth oxide thin films with a thickness of 0.50 渭m were deposited by thermal evaporation of bismuth oxide powders on glass substrates under a vacuum pressure of approximately 4-10 mbar. This was followed by doping the films with iron by mixing the iron nano-powders with the bismuth oxide powders before evaporation. The researcher used three increasing amounts of iron for this purpose.